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INFLUENCE OF BORON ON MICROSTRUCTURE AND MECHANICAL PROPERTIES OF RAPIDLY SOLIDIFIED Ni_3Al

LI Hui Institute of Metal Research , Academia Sinica , Shenyang , ChinaLIU Xiang Northeast Institute of Technology , Shenyang , ChinaGUO Jianting HU Zhuangqi Institute of Metal Research , Academia Sinica , Shenyang , China Associate Professor , Institute of Metall Research , Academia Sinica , Shenyang , China

金属学报(英文版)

By means of nonstoichiometry,rapid solidification and adequate boron addition,the tensile strength and bending resistance of Ni_3Al has been improved.When adding 0.52 to 1.37 at.-% B into Ni_3Al,which has the beneficial effect on the ductility.If boron addition is too high, there are coarse Ni_(23)B_6 particles and NiB_(12) phases found at the grain boundaries.Boron modification in Ni_3Al promotes the ordering in the region near grain boundaries.The grain boundary of boron free Ni_3Al is a large angle one,but turns into a small angle grain bound- ary with sub-grains of dislocation characteristics when the boron content in Ni_3Al reaches 1.37 at.-%.

关键词: intermetallic compound , null , null , null

MICROSTRUCTURE AND INDENTATION BEHAVIOUR OF MULTILAYER Ti-N FILM

WAGENDRISTEL A Viena Technical Univessity , AustriaHUANG Rongfang Institute of Metal Research , Academia Sinica , Shenyang , ChinaBANGERT H YANG Xia WU Lihang WANG Haifeng PANGRATZ H SKALICKY P Viena Technical University , Austria Associate Professor , Institute of Metall Research , Academia Sinica , Shenyang 110015 , China

金属学报(英文版)

The microstructure of Ti/TiN multilayer film was studied.It was shown by trans- mission electron microscopy of cross-sectional sample and respective secondary neutrals mass-spectroscopy depth profiling that the film has a periodic alternate multilayered structure:substrate /FeTi/Ti/Ti_2N/TiN/Ti_2N/Ti/Ti_2N/TiN...Ti/Ti_2N/TiN,where FeTi and Ti_2N were the transition layers formed during ion plating.Cross-sectional fracture surface of indentation samples had been obtained and studied with scanning electron microscopy.It was shown that the multilayer film deformed during indentation, formed an indentation pit and a pile-up of materials around the indentation pit.As the applied load increased deformation region extended beyond the film/substratc interface and into the substrate,the interlayer crack in the film and hole formation at the film /substrate interface were initiated.It is also shown that the multilayered Ti/TiN film offered better toughness in comparison with single layer TiN film.

关键词: multilayer Ti-N film , null , null

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